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Synthesis of[7,7‐2H2]epibrassinolide В. А. ХрипачNatalya B. KhripachVladimir N. Zhabinskii2007 год

Synthesis of [7,7‐2H2]epibrassinolide
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Аннотация: Abstract Synthesis of labelled epibrassinolide containing two deuterium atoms in a position which is not subjected to isotopic exchange is reported. Key transformations include preparation of 6,7‐seco steroidal diacid, its cyclization to a cyclic anhydride followed by a regioselective reduction with NaBD 4 . The obtained [7,7‐ 2 H 2 ]epibrassinolide can be used in biochemical experiments when the loss of isotopic label should be avoided. Copyright © 2007 John Wiley & Sons, Ltd.
Год издания: 2007
Авторы: В. А. Хрипач, Natalya B. Khripach, Vladimir N. Zhabinskii, Yuliya Y. Zhiburtovich, Bernd Schneider, C.P.G.M. de Groot
Издательство: Wiley
Источник: Journal of Labelled Compounds and Radiopharmaceuticals
Ключевые слова: Steroid Chemistry and Biochemistry, Phytochemical Studies and Bioactivities, Sesquiterpenes and Asteraceae Studies