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Strong hydrogen bondin the crystalstructure design ofCuNbOF5·4H2O Laptash N.M.Udovenko A.A.Vasiliev A.D.2023 год

Strong hydrogen bond in the crystal structure design of CuNbOF5·4H2O
статья из журнала

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База данных: Каталог библиотеки СФУ
Библиографическое описание: Strong hydrogen bond in the crystal structure design of CuNbOF5·4H2O : научное издание / N. M. Laptash [et al.]. - Текст : непосредственный // Journal of Solid State Chemistry. - 2023. - Т. 318, № . - P. 123781. - ISSN 0022-4596. - ISSN 1095-726X, DOI 10.1016/j.jssc.2022.123781.
Аннотация: Fluoride metal-organic frameworks (MOFs) based on pillared [NbOF5]2– anion have been recently received research attention as ultramicroporous materials for gas storage and separation. The trans-directing property of the NbOF5 octahedron plays a significant role in designing mixed metal oxyfluoride compounds composed of the alternating transition metal polyhedra, which are linked via oxide and fluoride ligands. Mixed metal CuNbOF5·4H2O is the only unique example when the trans-directing properties of [NbOF5]2– are realized in the formation of a strong O–H⋯F hydrogen bond (HB). Well-shaped single crystals of this compound were grown and their structure was refined by X-ray diffraction. Under quasi-isobaric conditions, a phase transition at 88 ​°C takes place, which is associated with the weakening of HBs and formation of ordinary chains through conventional trans-(O,F) bridges. The character of hydrogen bonding in CuNbOF5·4H2O affects its thermal behavior described by the dehydration and pyrohydrolysis processes.
Год издания: 2023
Авторы: Laptash N.M. , Udovenko A.A. , Vasiliev A.D. , Merkulov E.B.
Издательство: Academic Press
Источник: Journal of Solid State Chemistry
Выпуск: Т. 318
Номера страниц: 123781
Держатель оригинала документа: Institute of Chemistry, Far Eastern Branch of RAS, 159 Pr. Stoletiya Vladivostoka, 690022, Vladivostok, Russia, Kirensky Institute of Physics, Siberian Branch of RAS, Academgorodok, 660036, Krasnoyarsk, Russia
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